Curr Microbiol DOI 10.1007/s00284-014-0610-z Viable Intestinal Passage of a Canine Jejunal Commensal Strain Lactobacillus acidophilus LAB20 in Dogs

Yurui Tang• Per E. J. Saris

Received: 3 March 2014 / Accepted: 27 March 2014

Ó Springer Science+Business Media New York 2014

Abstract The strain Lactobacillus acidophilus LAB20

with immunomodulatory properties was previously found

dominant in the jejunal chyme of four dogs, and the novel

surface layer protein of LAB20 suggested its competitive

colonization in canine gut. To evaluate the persistence and

survival of LAB20 in healthy dogs, LAB20 was fed to five

healthy pet dogs for 3 days, at a dosage of 108 CFU daily as

fermented milk supplement. The fecal samples, from 1 day

prior to feeding, three continuous feeding days, and on day

5, 7, 14, and 21, were collected for strain-specific detection

of LAB20 using real-time PCR. We found that LAB20

count was significantly increased in dog fecal samples at

the second feeding day, but rapidly decreased after feeding

ceased. The fecal samples from prior to feeding, during

feeding, and post-cessation days were plated onto mLBS7

agar, from where LAB20 was recovered and distinguish-

able from other fecal lactobacilli based on its colony

morphotype. Using strain-specific PCR detection, the col-

onies were further verified as LAB20 indicating that

LAB20 can survive through the passage of the canine

intestine. This study suggested that canine-derived strain

LAB20 maintained at high numbers during feeding, viably

transited through the dog gut, and could be identified based

on its colony morphotype.

Introduction

In the gastrointestinal tract (GIT) of vertebrates, a dynamic

and sophisticated balance of microbial ecology is

Y. Tang P. E. J. Saris (&)

Department of Food and Environmental Sciences, University of

Helsinki, P. O. Box 56, 00014 Helsinki, Finland

e-mail: Per.Saris@helsinki.fi

established beginning at birth and continues to develop

throughout the life span of the host. The variation in host

dietary preference, age, lifestyle, and genetic background

shapes microbiota to be specific among individuals [5, 8,

31]. The microbiota inhabits the GIT, in turn, facilitates

nutrient digestion, and interacts with host by mediating

immune responses. Lactobacillus species are present

throughout the mammalian GIT [12, 36], and some Lac-

tobacillus strains are prevalently utilized in probiotic pro-

ducts. Probiotics are suggested to promote the health of

human and also animals, by preventing pathogen invasion,

producing antimicrobial substances, and enhancing the

immune responses [10]. Recent clinical studies have shown

that probiotics may be helpful to prevent or treat a variety

of acute and chronic gastrointestinal diseases, such as

antibiotic-associated diarrhea and inflammatory bowel

diseases [7, 24]. For companion animals, probiotics have

also been recommended to alleviate gut problem led by

intestinal dysbiosis [3, 37]. However, most canine probiotic

products contain human-derived strains [37]. With respect

to host specificity, probiotic strains with sufficient capa-

bility to adapt and colonize to the canine gut are needed.

Probiotics are typically transient residents in the intes-

tine, although probiotic strains show the ability to tolerate

and colonize the intestine both in vitro and in vivo [1, 11,

35, 38]. Therefore, it is intriguing to investigate how and

why endogenous bacteria could maintain themselves in the

GIT, and it may shed light to probiotic applications. There

have been a number of studies investigated the probiotic

effects of strains isolated from canine origin [2, 16–18, 21,

25]; however, most of those studies are confined to canine

fecal isolates. There is increasing number of supporting

evidence for that fecal microbiota differs from that in the

upper intestine [14, 19, 39]. O’Mahony et al. [20] isolated

commensal strains with probiotic potential from the large

123Y. Tang, P. E. J. Saris: Viable Intestinal Passage of Lactobacillus acidophilus LAB20

intestine of healthy canines, but only Bifidobacteria ani-

malis AHC7 was involved in the intervention study, which

reduced the carriage of Clostridia in dogs. To our knowl-

edge, there has been no intervention studies with Lacto-

bacillus strains derived from canine intestinal tract.

Previously, Tang et al. [29] presented the dominance of

L. acidophilus LAB20 in canine jejunal chyme of fistulated

dogs. Four out of five dogs harbored endogenous LAB20 as

dominant lactobacilli strain suggesting that this particular

strain could be a good candidate to investigate the possible

factors facilitating it to colonize and be predominant in dog

gut. Recently, LAB20 was found able to attenuate LPS-

induced interleukin-8 in HT-29 cells, suggesting the

potential probiotic properties of LAB20 to alleviate intes-

tinal problems associated with inflammation [30]. In the

present study, one aim was to evaluate if fed LAB20 can

persist in canine gut of healthy dogs, as suggested by Tang

and Saris’ previous study [28]. Another aim was to study if

endogenous LAB20 can survive the passage of the canine

intestine.

was stored at 4 °C before feeding, enumerated and exam-

ined by microscopy before delivery to the dog owners.

Feeding and Sample Handling

LAB20 was fed to dogs in fermented milk (3.4 9

106 CFU/ml, 50 ml per meal) with dog food. Five healthy

pet dogs (from 3 to 10 years old) from different owners

(breeds included Collie Smooth, Siberian husky, Welsh

corgi Pembroke, and Dogo argentino) were fed with

LAB20 supplementary for 3 days. Fresh fecal samples

were collected into a sterile Falcon tube after defecation

and stored in-20 °C. Samples were collected from 1 day

prior to LAB20 feeding and 3-day feeding period followed

by four collections at day 5, 7, 14, and 21. The sample

collection dates were chosen based on the results of the

previous study [28], and a shorter feeding period was

chosen because LAB20 showed highest copy numbers in

dog feces at feeding day 3 in the previous study. The study

was approved by the University of Helsinki ethics

committee.

Materials and Methods

Freeze Drying of LAB20 and Fermented Milk

Preparation

Lactobacillus acidophilus LAB20 was previously isolated

from canine jejunal chyme [29]. It was cultured in LBS

broth aerobically (BBL, Becton–Dickinson Microbiology

System, Cockeysville, MD, USA) without acetic acid and

pH adjusted to 7 with 5 M NaOH (mLBS7) to optimize

LAB20 growth.

Due to rather poor growth of LAB20 (106-7 CFU/ml in

mLBS in 18 h), LAB20 cells were concentrated and stored

as freeze-dried batches. For each batch of freeze-dried

bacteria, 400 ml mLBS7 broth was inoculated with over-

night LAB20 culture (1 % inoculum), and grown at 37°C

for 18 h. Bacterial cells were harvested by centrifugation at

16,000g for 10 min at 4 °C and washed twice with ice-cold

0.85 % NaCl. Bacterial cells were then resuspended in

5 ml of cryoprotectant (11 % w/v skim milk powder, 1 M

glycerol, 10 % w/v trehalose), five aliquots were let to

stand in room temperature for 10 min allowing equilibra-

tion between cells and cryoprotectant, and then lyophilized

in a Hetovac VR-1 (HETO Lab Equipment, Denmark).

Viability of bacteria was determined before and after

freeze-drying by serial dilution, and plated on mLBS7 plate

and incubated at 37 °C for 48 h. Freeze-dried LAB20 cells

were stored at 4 °C.

Approximately 107 CFU of LAB20 were inoculated into

50 ml sterilized (110°C 15 min) skimmed milk (10 %

w/v), and incubated at 37°C for 25 h. The fermented milk

DNA Extraction and Real-Time PCR Detection

Total genomic DNA of fecal samples was extracted using

QIAamp DNA stool kit (Qiangen Inc., Valencia, CA,

USA). The strain-specific real-time PCR detection was

performed according to the methods described by Tang and

Saris [28]. Briefly, serial dilutions of pLEB767, plasmid

carrying partial S-layer protein gene of LAB20, were used

for calibration. Primers RT1 and RT2 were designed to

specifically target 136 bp variation region of LAB20

S-layer gene. Real-time PCR was performed with Maxima

SYBR Green/ROX qPCR Master Mix (Thermo Scientific,

Helsinki, Finland) on the ABI Prism 7300 (Applied Bio-

systems, Foster City, CA).

Plate Fecal Samples and PCR Detection

According to real-time PCR results, the fecal samples with

highest LAB20 counts, together with the samples prior to

feeding, day 7, and day 21 samples from each dog (dog 2

did not defecate at day 21), were diluted with saline water

and plated on mLBS7 agar plates. After incubation at

37 °C for 2 days, the colony morphotype was inspected

and compared to LAB20. The colonies with similar mor-

photype to LAB20 were randomly picked and checked by

PCR, targeted to variable region of LAB20 S-layer protein.

In order to investigate the freeze and defreeze procedure on

the LAB20 viability, aliquot fecal sample at pre-feeding

day was spiked with LAB20 and plated with or without

freezing treatment.

123Y. Tang, P. E. J. Saris: Viable Intestinal Passage of Lactobacillus acidophilus LAB20

Fig. 1 Fecal LAB20 counts detected with strain-specific PCR

targeted to variable region of L. acidophilus LAB20 S-layer protein

gene. LAB20 fermented milk was fed (1.7 9 108 CFU daily) to dogs

from day 1 to day 3, and fecal samples were collected prior to feeding

and at days 1, 2, 3, 5, 7, 14, and 21. Dog 5 did not defecate at day 1,

and samples from dog 3 at day 14 and 21 could not be obtained from

owner. Data are generated from three fecal samples, respectively, and

expressed as means ± standard deviations

Statistical Analysis

Logarithms of fecal partial S-layer protein gene copy

numbers were used to achieve distribution of LAB20, and

analyzed using SPSS (IBM SPSS statistics 21) with one-

way ANOVA with time as the main factor; differences

among means of dogs were analyzed by the Student–

Newman–Keuls test. Differences were considered statisti-

cally significant at P \ 0.05.

Results

LAB20 Counts in Freeze-Dried Batch and Fermented

Milk

Due to rather poor growth, LAB20 cells were concentrated

and stored as freeze-dried batches. Approximately 107

CFU of LAB20 were inoculated into 50 ml sterilized

skimmed milk (10 % w/v), after 25 h incubation, the fer-

mented milk contained 3.4 9 106 CFU/ml LAB20. In

order to test the survival of LAB20 during storage, fer-

mented milk was stored at 4 °C for three days, the CFU of

LAB20 in fermented milk were counted daily. The result

showed that LAB20 counts remained nearly the same

during three days storage (data not shown).

Real-Time PCR Detection of LAB20 in Dog Fecal

Samples

To determine the LAB20 counts in dog feces during the

intervention study, strain-specific real-time PCR was used

targeting the variation region of LAB20 S-layer protein

gene. The gene copy number of LAB20 prior to the feeding

was set as the baseline for real-time PCR detection, and it

varied from 0 ± 0 to 102.98 ± 100.22 copies/g among

individual dogs. During the feeding period, LAB20 was

detected from fecal samples with significantly increased

numbers at day 2 and 3 compared to the following col-

lection days and prior to feeding (P \ 0.01). After the

feeding ceased, LAB20 counts were back to initial baseline

gradually except dog 1, in which LAB20 counts dropped to

baseline after second feeding day (Fig. 1). There was no

significant (P [ 0.05) difference among individual dogs

concerning the changing trend of LAB20 counts during the

collection period.

Storage and melting process could have lethal effect on

LAB20, which may lead to bias of the actual LAB20

counts in dog feces. Therefore, LAB20 was spiked to fecal

samples with or without freeze storage to study the effect

of storage and thawing on LAB20 in dog feces. Two ali-

quot fecal samples were spiked with 200 ll of LAB20

overnight culture. Without freezing and melting 3.15 9

106 CFU/g of LAB20 was obtained. Freezing at-20 °C

for two days and melting the sample before plating yielded

1.34 9 105 CFU/g LAB20.

LAB20 Colonies on Fecal Sample Plates

To determine if LAB20 can survive through canine gut, the

fecal samples at prior feeding, the day with highest LAB20

counts with real-time PCR, and samples at day 7 and 21

were plated on mLBS7 agar. By comparing with the prior

to feeding samples, the colony with unique morphotype

and similar to LAB20 was recognized from every feeding

123Y. Tang, P. E. J. Saris: Viable Intestinal Passage of Lactobacillus acidophilus LAB20

Fig. 2 Colonies formed on

mLBS7 agar from fecal samples

at same dilution (feces diluted

1049). a Colonies from fecal

sample of prior feeding day of

dog 2, and the colonies are

magnified in b. c Colonies from

fecal sample of feeding day 3 of

dog 2, and the colonies are

magnified in d (from further

tenfold dilution of the same

fecal sample, to give clear

image of colonies)

Fig. 3 PCR-amplified partial LAB20 S-layer protein gene from fecal

colonies. Lanes 1–8 fecal colonies from samples of dog 1. Lanes 9–17

fecal colonies from dog 2. Lanes 18–24 fecal colonies from dog 3.

Lanes 25–34 fecal colonies from dog 5. Lanes 35–41 fecal colonies

from dog 4. Lanes 42 is LAB20 as positive control. Underline symbol

‘‘

-’’ indicates the morphotype of colony on plate is different than

LAB20, whereas ‘‘?’’ represent the fecal colony morphotype similar

to LAB20 colony

123Y. Tang, P. E. J. Saris: Viable Intestinal Passage of Lactobacillus acidophilus LAB20

period plate of each dog. The colonies in prior to feeding

samples were replaced or outnumbered by LAB20-like

colonies from each dog feces samples of LAB20 feeding

day 2. The unique morphotype colony was rather flat and

with rough surface relative to other lactobacilli which were

less flat and had moist and smooth surface (Fig. 2). Colo-

nies from dog 1 are presented (Fig. 2), other plates were

found with similar results (not shown). To verify if the

unique morphotype colonies were LAB20, strain-specific

PCR was conducted. The colonies with different morpho-

types gave no amplification, whereas these unique colonies

yielded amplification with same size as LAB20 (Fig. 3).

Discussion

Lactobacilli are widely applied as probiotics to pursue its

desired beneficial effects on the hosts. Although many

probiotic strains present sufficient adhesion ability in vitro,

which is usually considered to contribute to the coloniza-

tion and persistence in the GIT, many of them fail to persist

in the GIT for long period [9, 15, 20, 38]. However,

identifying a probiotic with a reasonable persistence period

could represent a significant development, not only because

it could reduce the frequency of ingestion, but also because

it implies that the strain can adapt and thrive in the GIT.

Most probiotic strains and candidates are isolated from

fecal samples, but fecal isolates may just be transients

which fail to compete with endogenous inhabitants and

establish themselves in GIT. Furthermore, fecal isolates

mainly represent the microbiota in distal gut rather than

proximal gut [13, 19]. It has been shown that the pre-

existing microbial ecosystem is rather stable and resilient,

as it has been coevolved with the host over time [34].

Microbiome differences exist among individuals, due to

individual genetic background, immune response, and

dietary preferences [4, 22, 23, 26, 32], however, the met-

abolic end products are typically quite similar [32].

Therefore, a stable ecosystem is maintained as long as

microbial members of the community existing in GIT are

able to perform similar functions [6, 27]. This may explain

why it is strenuous for one single or a combination of

probiotic bacterial strains to integrate with pre-existing

ecosystem in the gut. Hence, it is intriguing to investigate

how the endogenous bacteria could maintain in the GIT,

especially the predominant ones, and may shed light on

probiotic applications.

Lactobacillus acidophilus LAB20 was previously found

predominant in canine jejunal lactobacilli, showed poten-

tial to persist in canine GIT for over six weeks post-

administration, and recently found with immunomodula-

tory properties [30]. Therefore, it was employed in the

present study to investigate its potential to persist and

transit through dog gut [29]. In this study, strain-specific real-

time PCR was used to detect LAB20 in dog feces, which was

previously validated [28]. Within three feeding days, LAB20

was detected with significantly (P \0.01) increased amount

in fecal samples, whereas dropped to baseline after feeding

ceased. The result suggests that LAB20 could transit through

dog gut during administration period. On the other hand, the

absence of LAB20 in following days indicated that either

LAB20 was unable to persist in canine gut, or it was diluted

to an undetectable amount in the feces, or it remained in the

canine gut and did not passage. Without access to the biopsy

samples, this could not be evaluated. However, in the study

of Valeur et al. [33], L. reuteri community in the stomach and

duodenum was found bigger than in fecal samples after

administration of human-derived L. reuteri ATCC 55730.

Further, by plating biopsy samples, no live L. reuteri were

found recovered on plates [33]. In another administration

study, Alander et al. [1] found that human-derived

L. rhamnosus GG generated from fecal samples may

underestimate colonization of probiotic strains in vivo.

Therefore, to determine whether LAB20 could colonize in

canine gut further investigation with biopsy samples is

needed.

The viability of LAB20 after transit through dog gut was

studied with plating assay. As the fecal samples had been

stored at-20 °C, the lethal effect of storage was first

determined. The result showed that the viability of LAB20

in feces reduced 20-fold during freezing and thawing

process. By plating fecal samples on mLBS7 agar, LAB20

was recovered from samples at feeding day which showed

abundant counts in real-time PCR, indicating LAB20 can

survive passage through dog gut (about 104–106 CFU/g of

feces). Interestingly, LAB20 colonies could be easily dis-

tinguished from that of other lactobacilli on mLBS7. By

comparing with the prior feeding samples, colonies with

unique morphotype similar to LAB20 were recognized

from each dog and further confirmed by LAB20-specific

PCR detection. Identification and quantification of LAB20

by colony morphotype inspection provides an easier way

than LAB20-specific real-time PCR to detect LAB20 sur-

viving the intestinal passage in future studies.

In conclusion, canine endogenous strain L. acidophilus

LAB20 was found able to survive at high numbers through

canine GIT during administration, and its colonies have

unique and distinguishable morphotype grown on the

mLBS7 agar plates. This feature of LAB20 facilitates the

future probiotic intervention studies, as its presence can be

monitored directly upon plating feces in the preliminary

inspections.

Acknowledgments We thank volunteers for providing dogs and

collecting fecal samples, Tuomas Puukko for kindly help to take the

bacterial colony photographs, and Dr. Timo M. Takala for his help in

123Y. Tang, P. E. J. Saris: Viable Intestinal Passage of Lactobacillus acidophilus LAB20

revision of this article. The authors would like to thank Viikki

Graduate School in Biosciences (VGSB) for study support, and

financial support from China Scholarship Council (CSC).

Conflict of interest of interest.

The authors declare that they have no conflict

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Maria Sempe